High-Resolution Thermal Expansion Measurements of Single-Crystal Sapphire for Application as X-Ray Backscattering Monochromator

ORAL

Abstract

We report measurements of the thermal expansion of high-purity single crystal sapphire along the $a$ and $c$ directions. The data were acquired using a thermal expansion cell that is constructed of fused silica with a relative resolution of approximately 3x10$^{-9}$. Comparison will be made to existing literature values determined from dilatometry and high-resolution x-ray diffraction. This project's main goal is the use of sapphire as x-ray backscattering monochromator for phonon spectroscopy using nuclear inelastic scattering. Tuning of the monochromator is done by varying the sapphire temperature, and the new thermal expansion values will improve the energy calibration.

Authors

  • John J. Neumeier

    Montana State University

  • I. Sergeev

    European Synchrotron Radiation Facility

  • D. Bessas

    Forschungszentrum Juelich

  • R.P. Hermann

    Forschungszentrum Juelich